Documentation:CHBE Exam Wiki/Module 3 - Separations 1

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CHBE 241
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Chemical and Biological Engineering
Welcome to the CHBE Exam Resources Wiki!

This wiki is intended to host past exams

with fully worked-out hints and solutions
Past Exams
Final Exam 2016W
Midterm Exam 1 2016W
Midterm Exam 2 2016W
Problem Sets
Module 1 - Process Basics
Module 2 - Reactors
Module 3 - Separations 1
Module 4 - Separations 2
Module 5 - Non-reactive Energy Balances
Module 6 - Reactive Energy Balances


Question 1

Convert the temperatures in parts (a) and (b) and temperature intervals in parts (c) and (d):
a) T=95°F to °R, °C,K

Solution


b) T=-50°C to K, °F, °R

Solution


c) ΔT=50°C to K, °F, °R

Solution


d) ΔT=120°R to °F, °C,K

Solution


Question 2

To regulate the temperature of a sand bath, a thermostat control with dial markings from 0 to 100 is used. A straight line that passes through the points (30, 300°F) and (90, 660°F) represents a calibration plot on the logarithmic coordinates of temperature (°F) versus dial setting,D.

Question 2a

Determine the equation for T in terms of D

Solution


Question 2b

What is the estimated dial setting to obtain 500°F?

Solution



Question 3

The following data was obtained from an experimental run,

x 0.5 1.4 11 35 54 72 84
y 2.1 4.2 4.9 5.4 5.8 6 6.25

Question 3a

Plot the data on logarithmic axes

Solution


Question 3b

Determine the coefficients of power law expression y =axb

Solution



Question 4

Calculate the pressure and gas-phase composition (mole fraction) in a system containing a liquid that is 0.5mol% N2 and 99.5 mol% water that is in equilibrium with nitrogen gas and water vapor at 90°C


Solution



Question 5

A mixture in the gaseous phase at 1 atm consisting of 40 mole% benzene and 60% toluene is cooled isobarically from an initial temperature of 115°C

CHBE 241 MOD 3 - Txy Benzene-toluene 1 atm

Question 5a

At what temperature does the first drop of condensate form?What is its composition?

Solution



Question 5b

Determine the mole fractions of benzene in the vapor and liquid phases when the temperature of the system is at 98°C.
What is the ratio (total moles in vapor/total moles in liquid) at this point.

Solution



Question 5c

At what temperature does the last bubble of vapor condense?What is its composition?

Solution



Question 6

A tank containing 50L of air-carbon tetrachloride gas mixture is at a temperature of 50°C, at an absolute pressure of 1.5 atm and a relative saturation of 40%.
To remove the CCl4 through gas adsorption, activated carbon is added to the tank. The volume of activated carbon can be assumed as negligible.


Question 6a

Calculate pCCl4 at the moment the tank is sealed, assuming ideal gas behavior and neglecting adsorption that occurs prior to sealing.

Solution


Question 6b

Calculate the total pressure in the tank and the partial pressure of carbon tetrachloride at a point when quarter of the CCl4 initially in the tank has been adsorbed.

Solution


Question 6c

How much activated carbon must be added to the tank to reduce the mole fraction of CCl4 in the gas to 0.001? Assume that the following relationship is true for the conditions in the tank

Solution



Question 7

A solution containing 100 lb KNO3 /100 lb H2O is cooled in a cooling crystallizer operating at 30°C. The slurry of from the crystallizer contains solid crystals suspended in saturated solution which then fed to a filter to separate the solid and liquid components.

Question 7a

Determine the production rate of crystals (lb /lb feed).

Solution


Question 7b

Determine the solid-to-liquid mass ratio of the slurry leaving the crystallizer

Solution